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Multivariate optimization of mebeverine analysis using molecularly imprinted polymer electrochemical sensor based on silver nanoparticles.
Nezhadali A, Bonakdar GA. Nezhadali A, et al. J Food Drug Anal. 2019 Jan;27(1):305-314. doi: 10.1016/j.jfda.2018.05.002. Epub 2018 Jun 6. J Food Drug Anal. 2019. PMID: 30648584 Free PMC article.
Two dynamic linear ranges of concentration for the MIP sensor were obtained as. 1 10 (-8) to 1 10 (-6) and 1 10 (-5) to1 10(-3) M with the limit of detection (LOD) of 8.6 10 (-9)M (S/N = 3). ...
Two dynamic linear ranges of concentration for the MIP sensor were obtained as. 1 10 (-8) to 1 10 (-6) and 1 10 (-5) to1 10(-3) M wit …
Determination of methimazole based on electropolymerized-molecularly imprinted polypyrrole modified pencil graphite sensor.
Nezhadali A, Mehri L, Shadmehri R. Nezhadali A, et al. Mater Sci Eng C Mater Biol Appl. 2018 Apr 1;85:225-232. doi: 10.1016/j.msec.2017.05.099. Epub 2017 May 17. Mater Sci Eng C Mater Biol Appl. 2018. PMID: 29407151
The accuracy of the method was studied through spiking blank samples showed recovery of 98% with precision of 4%. Limit of detection based on S/N=3 was obtained 310(-6)M. The proposed sensor was applied successfully to determine MMZ in biological model samples and pharmace …
The accuracy of the method was studied through spiking blank samples showed recovery of 98% with precision of 4%. Limit of detection based o …
Melamine Recognition: Molecularly Imprinted Polymer for Selective and Sensitive Determination of Melamine in Food Samples.
Biabani M, Nezhadali A, Nakhaei A, Nakhaei H. Biabani M, et al. Int J Anal Chem. 2020 Nov 1;2020:8864144. doi: 10.1155/2020/8864144. eCollection 2020. Int J Anal Chem. 2020. PMID: 33204272 Free PMC article.
Under the optimized conditions, an MIP sensor showed a linear range from 5.0 10(-7) to 1.0 10(-5) M MEL concentration with a correlation coefficient (R (2)) of 0.9997. The limit of detection was obtained (0.028 M) with a highly reproducible response (RSD 2.15%, n = …
Under the optimized conditions, an MIP sensor showed a linear range from 5.0 10(-7) to 1.0 10(-5) M MEL concentration with a correlat …
Spectrophotometric determination of fluoxetine by molecularly imprinted polypyrrole and optimization by experimental design, artificial neural network and genetic algorithm.
Nezhadali A, Motlagh MO, Sadeghzadeh S. Nezhadali A, et al. Spectrochim Acta A Mol Biomol Spectrosc. 2018 Feb 5;190:181-187. doi: 10.1016/j.saa.2017.09.021. Epub 2017 Sep 13. Spectrochim Acta A Mol Biomol Spectrosc. 2018. PMID: 28922645
At optimal condition the calibration curve showed linearity over a concentration range of 10(-7)-10(-8)M with a correlation coefficient (R(2)) of 0.9970. The limit of detection (LOD) for FLU was obtained 6.5610(-9)M. ...
At optimal condition the calibration curve showed linearity over a concentration range of 10(-7)-10(-8)M with a correlation coefficie …
Electrosynthesis of polypyrrole on steel fiber for solid-phase microextraction of citalopram in serum.
Nezhadali A, Ahmadi Bonakdar G, Nakhaei H. Nezhadali A, et al. Anal Bioanal Chem. 2012 Apr;403(2):593-600. doi: 10.1007/s00216-012-5825-x. Epub 2012 Feb 24. Anal Bioanal Chem. 2012. PMID: 22362278
The coating was prepared using a three-electrode electrochemical system from an acetonitrile/aqueous (ACN/H(2)O) oxalic acid solution containing 0.01 M of pyrrole monomer by applying a potential range (0-1.3 V) for 25 min. ...
The coating was prepared using a three-electrode electrochemical system from an acetonitrile/aqueous (ACN/H(2)O) oxalic acid solution contai …